HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)-tetradecanoic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | Tetradecanoic acid, 2-bromo-, ethyl ester | HCID 85791 | — |
| Product | 2-(4-Methoxy-phenylsulfanyl)-tetradecanoic acid ethyl ester | HCID 53881416 | 98% |
Reaction Steps
2-(4-Methoxy-phenylsulfanyl)-tetradecanoic acid ethyl ester was prepared according to the general method as outlined in Example 1. Starting from the corresponding ethyl -2-bromomyristate (5.0 g, 14.9 mmol) and 4-methoxythiophenol (1.9 g, 13.4 mmol), 5.0 g of the product was isolated. Yield 98%; Light yellow oil; MS: 393 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06172057B2 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-2565799a6b4b493bb253408260e54f05 |
| Source note | uspto-grants-2001_01 |