HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malononitrile → 2-(1-Ethoxypropylidene)malononitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | Ethyl orthopropionate | HCID 66995 | — |
| Product | 2-(1-Ethoxypropylidene)malononitrile | HCID 231470 | — |
Reaction Steps
16.41 g (249 mmol) of malononitrile and 43.8 g (249 mmol) of triethyl orthopropionate are refluxed for 4.5 hours. The reaction mixture is cooled to room temperature and distilled in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06174884B1 |
| Source dataset | uspto-grants-2001_01 |
| ORD ID | ord-5a7a2ebc62324adab460e8a1db82e678 |
| Source note | uspto-grants-2001_01 |