Sodium Acetate → HCID 178506542, compound
Reaction equation
[C:1]1([C:7]2[N:8]([CH2:12][CH2:13][CH2:14][NH2:15])[CH:9]=[CH:10][N:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[IH:16].CS[C:19]1[C:27]2[CH:28]=[CH:29][CH:30]=[C:25]3[C:26]=2[C:21](=[CH:22][CH:23]=[CH:24]3)[N:20]=1.C([O-])(=O)C.[Na+]>C(O)C>[IH:16].[C:1]1([C:7]2[N:8]([CH2:12][CH2:13][CH2:14][NH:15][C:19]3[C:27]4[CH:28]=[CH:29][CH:30]=[C:25]5[C:26]=4[C:21](=[CH:22][CH:23]=[CH:24]5)[N:20]=3)[CH:9]=[CH:10][N:11]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
A mixture of 4.0 g of 3-(2-phenyl-1H-imidazol-1-yl)propanamine, 6.5 g of 2-(methylthio)benz[cd]indole hydroiodide, 1.8 g of sodium acetate and 250 ml of ethanol was reacted as described in Example 11. The crude product was recrystallized from a mixture of ethanol and isopropanol giving 3.8 g of the desired product, mp 153° C.-155° C.