o-Fluorobenzaldehyde → o-Fluorostyrene

HRID 573470

Reaction equation

HRID 573470 reaction equation
[F:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH:4]=O.I[C:11]1C=CC=CC=1C=O>>[F:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH:4]=[CH2:11]

Participants

3

Reactant 2

HCID 67970o-FluorobenzaldehydeHCID 6434392-Iodobenzaldehyde

Product 1

HCID 123056o-FluorostyreneYield 20%

Procedure

The substantially same method as described in Preparation Example 284 was conducted, except that 2-fluorobenzaldehyde (Aldrich No. F4807) was used instead of 2-iodobenzaldehyde (Preparation Example 63) to obtain the title compound (1.82 g, yield 20˜40%).

Workup

  1. customThe substantially same method as described in Preparation Example 284

Sources & evidence

ORD record
ord-b57212672a994e3eb22d3222c568fa7c
Source dataset
uspto-grants-2015_05
Patent number
US09029589B2

Linked notes

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