HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylborane → Butyl ethyl(3-aminopropyl)phosphinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylborane | HCID 70400 | — |
| Reactant | Butyl ethyl(2-methyl-3-aminopropyl)phosphinate | HCID 46212766 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Butyl ethyl(3-aminopropyl)phosphinate | HCID 46212699 | 216.6% |
Reaction Steps
207 g (1 mol) of butyl ethyl(3-aminopropyl)phosphinate (produced as in Example 15) and 242 g (1 mol) of triphenylborane are stirred in 400 ml of toluene at room temperature for 1 hour. Toluene is distilled off at reduced pressure to leave 449 g (100% of theory) of butyl ethyl(3-aminopropyl)phosphinate as triphenylborane adduct.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09035088B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-c43a7e6d12634605955e22ca7a853a9c |
| Source note | uspto-grants-2015_05 |