HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloropyrimidine → 2-Chloro-4-(pyrimidin-2-ylthio)pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloropyrimidine | HCID 77531 | — |
| Reactant | HCID 178418793 | HCID 178418793 | — |
| Product | 2-Chloro-4-(pyrimidin-2-ylthio)pyrimidine | HCID 62344280 | 93.4% |
Reaction Steps
In a procedure analogous to Example 3, reaction of pyrimidine-2-thiol (415 mg, 3.70 mmol) and 2,4-dichloropyrimidine (500 mg, 3.36 mmol) furnished the product (705 mg, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09040549B2 |
| Source dataset | uspto-grants-2015_05 |
| ORD ID | ord-6dcd975089664cc1914ff8a9d3a29462 |
| Source note | uspto-grants-2015_05 |