Piperidin-2-ylmethanol → Cetyl chloroformate

HRID 579728

Reaction equation

HRID 579728 reaction equation
N1CCCC(CO)C1.N1CCCCC1CO.[Cl:17][C:18]([O:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36]CC)=[O:19]>>[Cl:17][C:18]([O:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36])=[O:19]

Participants

4

Reactant 3

HCID 94263Piperidin-2-ylmethanolHCID 103922Carbonochloridic acid, octadecyl esterHCID 107308Piperidin-3-ylmethanol

Product 1

HCID 97633Cetyl chloroformate

Procedure

Following essentially the procedure of Example 1(a), and using in place of 3-piperidinemethanol, an approximately equivalent amount of 2-piperidinemethanol, and using in place of octadecyl chloroformate, an approximately equivalent amount of hexadecyl chloroformate, a white solid was obtained.

Sources & evidence

ORD record
ord-4f545b215ed54ce5b61f414f9a28f90a
Source dataset
uspto-grants-1988_06
Patent number
US04749696

Linked notes

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