HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane → Benzene, 1-fluoro-2-(trifluoromethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane | HCID 20134582 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Benzene, 1-fluoro-2-(trifluoromethyl)- | HCID 9807 | 41% |
Reaction Steps
The general procedure was followed using 11.0 g of 1-vinyl-2-trifluoromethyl-2,3,3-trifluorocyclobutane dissolved in 11.15 g of benzene as the liquid feed at a flow rate of 1 ml/hr. Nitrogen was used as the inert carrier. The reactor was charged with 2.0 g of activated carbon. At 400° C. 41% of o-trifluoromethylfluorobenzene was produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04754084 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-39825371865942a4b6ee94c2fdc6ef8a |
| Source note | uspto-grants-1988_06 |