Morpholine → HCID 178513121, compound
Reaction equation
I.[NH:2]([C:4](SC)=[NH:5])[NH2:3].[NH:8]1[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1>CO>[N:8]1([C:4](=[NH:5])[NH:2][NH2:3])[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
To a solution of methyl hydrazinecarbimidothioate hydroiodide (0.100 g, 0.429 mmol) in MeOH (2 mL) was added morpholine (0.075 mL, 0.858 mmol) and refluxed overnight. Reaction was cool to RT and concentrated to get morpholine-4-carboximidhydrazide as a white solid in quantitative yield.
Workup
- temperaturerefluxed overnight
- customReaction
- concentrationconcentrated
Sources & evidence
- ORD record
- ord-6407090cb11347459dd3c8c7f1ae4f0f
- Source dataset
- uspto-grants-2016_01
- Patent number
- US09227971B2
Reaction notes
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