Sulfuryl chloride → 2,6-Dimethoxybenzenesulfonyl chloride

Reaction equation

Br[C:2]1[C:7]([O:8][CH3:9])=[CH:6][CH:5]=[CH:4][C:3]=1[O:10][CH3:11].[S:12](Cl)([Cl:15])(=[O:14])=[O:13]>>[CH3:11][O:10][C:3]1[CH:4]=[CH:5][CH:6]=[C:7]([O:8][CH3:9])[C:2]=1[S:12]([Cl:15])(=[O:14])=[O:13]

Participants

Reactant 2

HCID 24648Sulfuryl chloride

HCID 6122962-Bromo-1,3-dimethoxybenzene

Product 1

HCID 154110502,6-Dimethoxybenzenesulfonyl chloride

Procedure

2,6-Dimethoxybenzenesulfonyl chloride was prepared from 2-bromo-1,3-dimethoxybenzene according to the procedure in Example 1, Step 1. The reaction gave a mixture of sulfonyl chloride and another product as a white solid.

Workup

customThe reaction gave

Sources & evidence

ORD record: ord-5ef0ad4d861643f1848796d3d60755f5
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07906548B2

Reaction notes

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