HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → 2,5,5-Trimethyl-2-propyl-1,3-dioxane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 2-Pentanone | HCID 7895 | — |
| Reactant | Neopentyl glycol | HCID 31344 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2,5,5-Trimethyl-2-propyl-1,3-dioxane | HCID 79462 | — |
Reaction Steps
2-Pentanone, 2,2-dimethyl-propane-1,3-diol, and a catalytic amount of p-toluenesulfonic acid (PTSA) were refluxed in toluene to provide a crude product. Distillation provided the product 2,5,5-trimethyl-2-propyl-[1,3]dioxane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09441185B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-e5d10747c1d04c2695967de07f2120ed |
| Source note | uspto-grants-2016_09 |