2-Pentanone, 5-bromo- → HCID 20371482, compound

HRID 616221

Reaction equation

HRID 616221 reaction equation
[CH:1]1[C:11]2[CH:10]=[CH:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[C:6](=[C:16]3[CH2:21][CH2:20][NH:19][CH2:18][CH2:17]3)[C:5]=2[CH:4]=[CH:3][CH:2]=1.Br[CH2:23][CH2:24][CH2:25][C:26](=[O:28])[CH3:27]>>[CH:1]1[C:11]2[CH:10]=[CH:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[C:6](=[C:16]3[CH2:17][CH2:18][N:19]([CH2:23][CH2:24][CH2:25][C:26](=[O:28])[CH3:27])[CH2:20][CH2:21]3)[C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 774932-Pentanone, 5-bromo-HCID 1597184-(5H-Dibenzo(a,d)cyclohepten-5-ylidene)piperidine

Product 1

HCID 20371482HCID 20371482, compound

Procedure

4-(5-dibenzo[a,d]cycloheptenylidene)piperidine is reacted in a manner analogous to that described in Example 7 with 5-bromo-2-pentanone. M.P. of the hydrochloride of the title compound 206°-207° after crystallization from isopropanol.

Workup

  1. customM.P. of the hydrochloride of the title compound 206°-207° after crystallization from isopropanol

Sources & evidence

ORD record
ord-3d7f1cad167e4fb5bb6e19fe51c544a6
Source dataset
uspto-grants-1978_02
Patent number
US04072756

Linked notes

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