1,3-Dioxan-5-ol, 2-phenyl- → HCID 66834150, compound

HRID 61704

Reaction equation

HRID 61704 reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][C:5]2[C:17](=[O:18])[C:16]3[C:15]4[C:10](=[CH:11][C:12]([C:19]#[N:20])=[CH:13][CH:14]=4)[NH:9][C:8]=3[C:7]([CH3:22])([CH3:21])[C:6]=2[CH:23]=1.[C:24]1([CH:30]2[O:35][CH2:34][CH:33](O)[CH2:32][O:31]2)[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[CH3:22][C:7]1([CH3:21])[C:8]2[NH:9][C:10]3[C:15](=[CH:14][CH:13]=[C:12]([C:19]#[N:20])[CH:11]=3)[C:16]=2[C:17](=[O:18])[C:5]2[CH:4]=[CH:3][C:2]([O:1][CH:33]3[CH2:32][O:31][CH:30]([C:24]4[CH:25]=[CH:26][CH:27]=[CH:28][CH:29]=4)[O:35][CH2:34]3)=[CH:23][C:6]1=2

Participants

3

Reactant 2

HCID 743621,3-Dioxan-5-ol, 2-phenyl-HCID 668338618-Hydroxy-6,6-dimethyl-11-oxo-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile

Product 1

HCID 66834150HCID 66834150, compound

Procedure

Under the same conditions as the method for synthesizing Compound A7-1, the title compound was prepared from Compound A6 and 2-phenyl-[1,3]dioxan-5-ol.

Workup

  1. customUnder the same conditions as the method for synthesizing Compound A7-1

Sources & evidence

ORD record
ord-b8fd2d5e5b9c4b64aee253d24747981b
Source dataset
uspto-grants-2016_09
Patent number
US09440922B2

Linked notes

Loading…