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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 61822Generated: October 26, 2026

m-Chlorophenylhydrazine hydrochloride → 3-Chloro-8-methoxy-6,6-dimethyl-5,6-dihydrobenzo[b]carbazol-11-one

https://huagongshe.com/reaction/61822

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chlorophenylhydrazine hydrochlorideHCID 75331—
Reactant7-Methoxy-1,1-dimethyl-3,4-dihydronaphthalen-2(1H)-oneHCID 13011007—
Reactant3-Bromo-8-methoxy-6,6-dimethyl-5,6-dihydrobenzo[b]carbazol-11-oneHCID 66834292—
Product3-Chloro-8-methoxy-6,6-dimethyl-5,6-dihydrobenzo[b]carbazol-11-oneHCID 66834792—

Reaction Steps

Under the same conditions as the method for synthesizing Compound A3-1 and Compound A4, the title compound was prepared as a crude product from Compound A2 and (3-chlorophenyl)-hydrazine hydrochloric acid salt.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09440922B2
Source datasetuspto-grants-2016_09
ORD IDord-0f35be01de184ffbb4a7bc8c5d9114eb
Source noteuspto-grants-2016_09