N-(3-(3,6-dibromo-9H-carbazol-9-yl)propyl)aniline → N-(2-(oxiran-2-yl)ethyl)aniline

Reaction equation

[N+](C1C=CC=CC=1S([N:13]([CH2:20][CH2:21][CH:22]1[CH2:24][O:23]1)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)(=O)=O)([O-])=O.BrC1C=CC2N(CCCNC3C=CC=CC=3)C3C(C=2C=1)=CC(Br)=CC=3>>[O:23]1[CH2:24][CH:22]1[CH2:21][CH2:20][NH:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

Reactant 2

HCID 46851212N-(3-(3,6-dibromo-9H-carbazol-9-yl)propyl)aniline

HCID 580971922-nitro-N-(2-(oxiran-2-yl)ethyl)-N-phenylbenzenesulfonamide

Product 1

HCID 18628254N-(2-(oxiran-2-yl)ethyl)aniline

Procedure

Prepared from 2-nitro-N-(2-(oxiran-2-yl)ethyl)-N-phenylbenzenesulfonamide using an analogous procedure as used to prepare the compound of Example 20.

Sources & evidence

ORD record: ord-2080dcd089cf49b39f1edf028f58be26
Source dataset: uspto-grants-2016_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09446042B2

Reaction notes

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