HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-1,1,1-trifluoropropane → 2-(3,3,3-Trifluoro-propylsulfanyl)-nicotinic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-1,1,1-trifluoropropane | HCID 2725114 | — |
| Reactant | HCID 178524460 | HCID 178524460 | — |
| Product | 2-(3,3,3-Trifluoro-propylsulfanyl)-nicotinic acid | HCID 62033693 | 10% |
Reaction Steps
2-Mercapto-nicotinic acid (1 g, 6.4 mmol) and 3-bromo-1,1,1-trifluoropropane were reacted in the same manner as in Step A of Preparation Example 10 to obtain the title compound (0.16 g, 10%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09447044B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-1c1801a6c51a4b27bf71e7c919c5b737 |
| Source note | uspto-grants-2016_09 |