HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → HCID 178418677, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178418594 | HCID 178418594 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178418677 | HCID 178418677 | — |
Reaction Steps
0.1 mol of 2,3-difluoro-4-(trans-4-pentylcyclohexyl)methoxyphenol, 0.11 mol of butyl bromide and 0.11 mol of potassium carbonate are heated for 16 hours at 100° in 100 ml of dimethylformamide (DMF). After cooling, the inorganic salts are filtered off with suction, the filtrate is concentrated, and water is added. 1-butyloxy-2,3-difluoro-4-(trans-4-pentylcyclohexyl)methoxybenzene is obtained by extraction with dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05248447 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-709fc48404a84ef09737b5887db2472e |
| Source note | uspto-grants-1993_09 |