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1,4-Butanedisulfonyl dichloride → HCID 86756470, compound

HRID 636784
Notes
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Reaction equation

HRID 636784 reaction equation
[CH2:1]([S:9]([Cl:12])(=[O:11])=[O:10])[CH2:2][CH2:3][CH2:4][S:5]([Cl:8])(=[O:7])=[O:6].[NH2:13][C:14]1[CH:19]=[C:18]([SH:20])[C:17]([NH2:21])=[CH:16][C:15]=1[SH:22]>>[NH2:13][C:14]1[CH:19]=[C:18]([SH:20])[C:17]([NH2:21])=[CH:16][C:15]=1[SH:22].[CH2:1]([S:9]([Cl:12])(=[O:10])=[O:11])[CH2:2][CH2:3][CH2:4][S:5]([Cl:8])(=[O:7])=[O:6]
ParticipantsProcedureSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 3153171,4-Butanedisulfonyl dichloride2×HCID 45983552,5-Diamino-1,4-benzenedithiol

Product 1

HCID 86756470HCID 86756470, compound

Procedure

Next, the 1,4-butanedisulfonyl chloride vapor in the condensing chamber 2 was adiabatically expanded, and the introduced base particles were exposed thereto for 8 minutes. Consequently, a polymerization reaction between 2,5-diamino-1,4-benzenedithiol and 1,4-butanedisulfonyl chloride took place on the surface of the base particles, forming a film of 2,5-diamino-1,4-benzenedithiol-1,4-butanedisulfonyl chloride co-polymer.

Sources & evidence

ORD record
ord-96d8a162706048ceb64711578af2f2ec
Source dataset
uspto-grants-2001_02
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US06194487B1

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes