Sodium Azide → Methyl 1-(4-azidobutyl)cyclopentane-1-carboxylate

Reaction equation

[CH3:1][O:2][C:3]([C:5]1([CH2:10][CH2:11][CH2:12][CH2:13]Br)[CH2:9][CH2:8][CH2:7][CH2:6]1)=[O:4].[N-:15]=[N+:16]=[N-:17].[Na+]>>[CH3:1][O:2][C:3]([C:5]1([CH2:10][CH2:11][CH2:12][CH2:13][N:15]=[N+:16]=[N-:17])[CH2:9][CH2:8][CH2:7][CH2:6]1)=[O:4]

Participants

Reactant 2

HCID 33557Sodium Azide

HCID 229543431-(4-Bromobutyl)cyclopentanecarboxylic acid methyl ester

Product 1

HCID 23384160Methyl 1-(4-azidobutyl)cyclopentane-1-carboxylate

Procedure

The title compound was prepared using a similar procedure as described in Example 1, Step 2, starting from 1-[4-bromobutyl]cyclopentanecarboxylic acid methyl ester and sodium azide.

Sources & evidence

ORD record: ord-3bb84808d742487498f1b913a3b01372
Source dataset: uspto-grants-2016_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09447035B2

Reaction notes

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