(2-Aminoethyl)(benzyl)methylamine → HCID 178484236, compound
Reaction equation
[NH2:1][CH2:2][CH2:3][N:4]1[C:8]2[CH:9]=[CH:10][C:11](Cl)=[C:12]3[C:13](=[O:36])[C:14]4[C:19]([C:6]([C:7]=23)=[N:5]1)=[C:18]([O:20]CC1C=CC=CC=1)[CH:17]=[CH:16][C:15]=4[O:28]CC1C=CC=CC=1.[CH3:38][N:39](CC1C=CC=CC=1)[CH2:40][CH2:41][NH2:42]>>[NH2:1][CH2:2][CH2:3][N:4]1[C:8]2[CH:9]=[CH:10][C:11]([NH:42][CH2:41][CH2:40][NH:39][CH3:38])=[C:12]3[C:13](=[O:36])[C:14]4[C:19]([C:6]([C:7]=23)=[N:5]1)=[C:18]([OH:20])[CH:17]=[CH:16][C:15]=4[OH:28]Participants
3
Procedure
Reaction of 2-(2-aminoethyl)-5-chloro-7,10-bis-(phenylmethoxy)anthra[1,9-cd]pyrazol-6(2H)-one with N-methyl-N-(phenylmethyl)-1,2-ethanediamine as described in Example 78 gives the product; mp 169°-172° C.
Workup
- customgives the product
Sources & evidence
- ORD record
- ord-83bd628b8956460984fe623fa961f6a9