Cyclohexylamine → 8-Methylnonanoic acid cyclohexylamine salt

HRID 643199

Reaction equation

HRID 643199 reaction equation
[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10].[CH:13]1([NH2:19])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1>CCCCCCC>[CH:13]1([NH2:19])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1.[CH3:1][CH:2]([CH3:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10]

Participants

4

Reactant 2

HCID 7965CyclohexylamineHCID 1114708-Methylnonanoic acid

Product 1

HCID 686053248-Methylnonanoic acid cyclohexylamine salt

Reagents, catalysts & solvents 1

HCID 8900HeptaneSolvent

Procedure

From the 8-methylnonanoic acid crude product obtained in Example 1, 8.00 g was dissolved in heptane (30 ml). Cyclohexylamine (6.91 ml, 60.4 mmol) was slowly added dropwise at 0° C. (ice bath), and the mixture was stirred at room temperature for 20 minutes. The reaction mixture was filtered to give 8-methylnonanoic acid cyclohexylamine salt (15.7 g).

Workup

  1. filtrationThe reaction mixture was filtered

Sources & evidence

ORD record
ord-f0e91b54879e4f9caeab73e5e708080f
Source dataset
uspto-grants-2010_04
Patent number
US07700331B2

Linked notes

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