HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → Allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Allyl Alcohol | HCID 7858 | — |
| Reactant | 2-[4-(2-Quinoxalinyloxy)phenoxy]propionyl chloride | HCID 13670532 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate | HCID 13670534 | — |
Reaction Steps
To a solution of 1.2 g allyl alcohol and 1.6 g pyridine in 50 cc methylene chloride, add 6.6 g of 2-[4-(2-quinoxalinyloxy)phenoxy]propionyl chloride in 60 cc methylene chloride. Stir the mixture at room temperature overnight. Wash the methylene chloride solution with water and dry the solution over magnesium sulfate concentrate under vacuum to give allyl 2-[4-(2-quinoxalinyloxy)phenoxy]propanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04609396 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-a9135ae31a7f4357adf017005813a8cd |
| Source note | uspto-grants-1986_09 |