HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dibromo-5,5-dimethylhydantoin → 6-Bromo-2,3-dimethoxybenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dibromo-5,5-dimethylhydantoin | HCID 6479 | — |
| Reactant | 2,3-Dimethoxybenzoic acid | HCID 15204 | — |
| Product | 6-Bromo-2,3-dimethoxybenzoic acid | HCID 11054430 | — |
Reaction Steps
Using the procedure described herein above in Example 1, Method E, 2,3-dimethoxybenzoic acid was brominated with DBDMH to provide the following results (assay yields) after reacting for 22 hours at 20°-25° C:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05248817 |
| Source dataset | uspto-grants-1993_09 |
| ORD ID | ord-4583e7f0d868404ea0bdbff4012d8e64 |
| Source note | uspto-grants-1993_09 |