HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → Diepoxyoctane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1,2:7,8-Diepoxyoctane | HCID 17048 | — |
| Product | Diepoxyoctane | HCID 21943853 | — |
Reaction Steps
A 1-liter resin flask was charged with 200 g of PEG-7500 and 0.3 g KOH and vacuum stripped at 100° C. for one-half hour. To this stirred solution under nitrogen were added 5.5 g of 1,2,7,8-diepoxyoctane at 100° C. over 15 minutes. The mixture was maintained at this temperature for an additional one and one-half hours followed by quenching with 250 g of water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04411775 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-8891115a7a3b41ce8053755280664e69 |
| Source note | uspto-grants-1983_10 |