Cesium fluoride → Allyl Oxalofluoride

HRID 649255

Reaction equation

HRID 649255 reaction equation
[CH2:1]([O:4][C:5](=[O:9])[C:6](Cl)=[O:7])[CH:2]=[CH2:3].[F-:10].[Cs+]>>[CH2:1]([O:4][C:5](=[O:9])[C:6]([F:10])=[O:7])[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 25953Cesium fluorideHCID 3018516Allyl chlorooxoacetate

Product 1

HCID 14153244Allyl Oxalofluoride

Procedure

By the procedure of the preceding Preparation, allyl oxalochloride (252.5 g, 1.70 mol) and cesium fluoride (284 g, 1.87 mol) were converted to twice distilled title product, b.p. 48°-50° C./35 mm; 124°-126° C. (atmospheric pressure).

Workup

  1. distillationto twice distilled title product, b.p. 48°-50° C./35 mm
  2. custom124°-126° C. (atmospheric pressure)

Sources & evidence

ORD record
ord-e0232b6b3e3e495ca8bd281a4b73c66e
Source dataset
uspto-grants-1988_04
Patent number
US04739047

Linked notes

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