Cyclohexanone → 3-Phenyl-1-methyl-4-cyclohexyl-5-pyrazolamine

HRID 65016

Reaction equation

HRID 65016 reaction equation
[C:1]1([N:7]2[C:11]([NH2:12])=[CH:10][C:9]([CH3:13])=[N:8]2)C=CC=CC=1.[C:14]1(=O)[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]1>>[C:13]1([C:9]2[C:10]([CH:14]3[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]3)=[C:11]([NH2:12])[N:7]([CH3:1])[N:8]=2)[CH:18]=[CH:19][CH:14]=[CH:15][CH:16]=1

Participants

3

Reactant 2

HCID 7967CyclohexanoneHCID 708015-Amino-3-methyl-1-phenylpyrazole

Product 1

HCID 202349793-Phenyl-1-methyl-4-cyclohexyl-5-pyrazolamine

Procedure

It is obtained by following essentially the procedure of example 1, reacting 1-phenyl-3-methyl-5-pyrazolamine with cyclohexanone (1:2, molar ratio) at a temperature of about 45° C. for about 8 hours. M.p. 212°-214° C.

Workup

  1. customIt is obtained
  2. customat a temperature of about 45° C.
  3. customfor about 8 hours

Sources & evidence

ORD record
ord-36b46232b8b14df5927b27ad5f8f8603
Source dataset
uspto-grants-1986_09
Patent number
US04612318

Linked notes

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