HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → 6-(2-Chlorophenyl)-3-(4-oxopiperidino)-1,2,4-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Piperonylamine | HCID 2723901 | — |
| Reactant | 3-Chloro-6-(o-chlorophenyl)-1,2,4-triazine | HCID 12581288 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-(2-Chlorophenyl)-3-(4-oxopiperidino)-1,2,4-triazine | HCID 13605527 | — |
Reaction Steps
1.5 g of 3-chloro-6-(2-chlorophenyl)-1,2,4-triazine, 3.05 g of piperidin-4-one monohydrate hydrochloride and 3.1 g of sodium carbonate are heated under reflux in 100 ml of ethanol for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04613603 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-bde75dd99363429981065e3c265be9d8 |
| Source note | uspto-grants-1986_09 |