HCID 18962534, compound → HCID 11745175, compound

Reaction equation

C([O:8][C:9]1[C:17]([O:18][CH2:19]C)=[CH:16][CH:15]=[C:14]2[C:10]=1[CH:11]=[C:12]([CH3:21])[NH:13]2)C1C=CC=CC=1.C(OC1C(OC)=CC=C2C=1C=C(C)N2)C1C=CC=CC=1>>[OH:8][C:9]1[C:17]([O:18][CH3:19])=[CH:16][CH:15]=[C:14]2[C:10]=1[CH:11]=[C:12]([CH3:21])[NH:13]2

Participants

Reactant 2

HCID 18962534HCID 18962534, compound

HCID 18962540HCID 18962540, compound

Product 1

HCID 11745175HCID 11745175, compoundYield 89%

Procedure

This compound is obtained according to the operating method described in Example 2c, in which the 4-benzyloxy-5-ethoxy-2-methylindole is replaced by 4-benzyloxy-5-methoxy-2-methylindole. Following the operating method of Example 2 a pale yellow powder is obtained (yield=89%, m.p.=118°-119° C.).

Workup

customThis compound is obtained
customis obtained (yield=89%, m.p.=118°-119° C.)

Sources & evidence

ORD record: ord-8c34ac0688e54e8aae1df14761c59498
Source dataset: uspto-grants-1992_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05131911

Reaction notes

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