HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 654459Generated: October 27, 2026
5-Chloro-2-nitrobenzoic acid → 5-Chloro-2-nitrobenzoyl chloride
https://huagongshe.com/reaction/654459
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 5-Chloro-2-nitrobenzoyl chloride | HCID 2723685 | — |
Reaction Steps
A mixture of 80.6 g of 5-chloro-2-nitrobenzoic acid and 58.2 ml of thionyl chloride is heated at 90° C. for 2 hours. The excess thionyl chloride is then distilled off in vacuo. 87.1 g of 5-chloro-2-nitrobenzoyl chloride are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05132314 |
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| Source dataset | uspto-grants-1992_07 |
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| ORD ID | ord-a77377dc679e46d883508eddd15de74a |
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| Source note | uspto-grants-1992_07 |
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