1,6-Hexanediol → 1-Isocyanatoheptadecane

HRID 654831

Reaction equation

HRID 654831 reaction equation
[CH2:1](O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]O.[CH2:9]([N:24]=[C:25]=[O:26])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19]CCCC>C(O)COCCO>[CH2:9]([N:24]=[C:25]=[O:26])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH3:1]

Participants

4

Reactant 2

HCID 123741,6-HexanediolHCID 14464675Pentadecyl isocyanate

Product 1

HCID 135601031-Isocyanatoheptadecane

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

Following the procedure described in preparation 4, but using 1,6-hexanediol and n-pentadecylisocyanate, instead of diethylene glycol and n-heptadecylisocyanate respectively, the title compound was obtained in a similar yield.

Workup

  1. customdescribed in preparation 4

Sources & evidence

ORD record
ord-5d87856d36764e5f9e9ae663930d0805
Source dataset
uspto-grants-1992_07
Patent number
US05134151

Linked notes

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