Thiodiglycol → 1-Isocyanatoheptadecane

HRID 654832

Reaction equation

HRID 654832 reaction equation
[CH2:1](O)[CH2:2]SCCO.[CH2:8]([N:23]=[C:24]=[O:25])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>C(O)COCCO>[CH2:8]([N:23]=[C:24]=[O:25])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:1][CH3:2]

Participants

4

Reactant 2

HCID 5447ThiodiglycolHCID 14464675Pentadecyl isocyanate

Product 1

HCID 135601031-Isocyanatoheptadecane

Reagents, catalysts & solvents 1

HCID 8117Diethylene GlycolSolvent

Procedure

Following the procedure described in preparation 4, but using thiodiethylene glycol and n-pentadecylisocyanate, instead of diethylene glycol and n-heptadecylisocyanate, respectively, the title compound of this preparation was obtained in a similar yield.

Workup

  1. customdescribed in preparation 4

Sources & evidence

ORD record
ord-b2b87a204768457a8a631807a9470e01
Source dataset
uspto-grants-1992_07
Patent number
US05134151

Linked notes

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