HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hypochlorite → Sodium 3,3-dimethyl-2-oxobutyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hypochlorite | HCID 23665760 | — |
| Reactant | Sodium 3,3-dimethyl-2-hydroxybutyrate | HCID 23694960 | — |
| Catalyst | Ruthenium dioxide hydrate | HCID 16211523 | — |
| Solvent | Water | HCID 962 | — |
| Product | Sodium 3,3-dimethyl-2-oxobutyrate | HCID 23674764 | — |
Reaction Steps
Sodium 3,3-dimethyl-2-hydroxybutyrate and ruthenium dioxide hydrate are added to water, the pH rendered alkaline, and sodium hypochlorite is slowly added to produce sodium 3,3-dimethyl-2-oxobutyrate in high yield and purity. The solid catalyst is filtered off and may be re-used while the filtrate can be directly used in further synthesis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04614822 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-0abcb0c150bc4175a08041240e6ed897 |
| Source note | uspto-grants-1986_09 |