HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylcyclohexanone → Methyl 3-(1-methyl-2-oxocyclohexyl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylcyclohexanone | HCID 11419 | — |
| Reactant | 2-Methylcyclopentanone | HCID 14265 | — |
| Reactant | 1-Methyl-2-oxocyclopentanepropionic acid methyl ester | HCID 12291889 | — |
| Product | Methyl 3-(1-methyl-2-oxocyclohexyl)propanoate | HCID 574325 | — |
Reaction Steps
In the same manner but replacing 2-methylcyclohexanone with an equivalent amount of 2-methylcyclopentanone, 1-methyl-2-oxocyclopentanepropionic acid methyl ester, bp 88°-100° C./1.1 mm, nmr (CDCl3) δ 1.0 (s, 3H), 1.8 (m, 6H), 2.3 (m, 4H), 3.7 (s, 3H), is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04128560 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-0ac5163d69744a34a58712d9781fbae8 |
| Source note | uspto-grants-1978_12 |