HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Chloro-3-fluoroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Chloro-1-fluoro-3-nitrobenzene | HCID 88883 | — |
| Product | 2-Chloro-3-fluoroaniline | HCID 88884 | — |
Reaction Steps
19.6 g. of 2-chloro-3-fluoronitrobenzene (0.11 mole) is reduced with stannous chloride (118 g., 0.63 mole) in 180 ml. of concentrated hydrochloric acid. The solution is basified with aqueous sodium hydroxide and extracted with chloroform to yield 2-chloro-3-fluoroaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04128666 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-1db00a5a9136416fb08e3a530f59cd2f |
| Source note | uspto-grants-1978_12 |