Hexamethylenetetramine → Molybdenum hexamethylenetetramine
Reaction equation
[CH2:1]1[N:6]2[CH2:7][N:8]3[CH2:10][N:4]([CH2:5]2)[CH2:3][N:2]1[CH2:9]3.O[Mo:12](O)(=O)=O.[NH4+].[NH4+].[O-][Mo]([O-])(=O)=O>O>[Mo:12].[CH2:1]1[N:6]2[CH2:7][N:8]3[CH2:10][N:4]([CH2:5]2)[CH2:3][N:2]1[CH2:9]3Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
Hexamethylenetetramine molybdate having a 2/1 molybdenum/hexamethylenetetramine molar ratio was prepared as follows. 10 grams of hexamethylenetetramine was dissolved in 100 ml water heated near reflux temperature. 24.01 grams of commercial, so-called "molybdic acid" (actually at least one ammonium molybdate) was dissolved in 169 ml water heated to reflux temperature. The first solution was added to the second solution.
Workup
- temperatureheated
- temperaturenear reflux temperature
- temperatureheated
- temperatureto reflux temperature
- additionThe first solution was added to the second solution
Sources & evidence
- ORD record
- ord-242010b0e43b497ba711f280db016fe8
- Source dataset
- uspto-grants-1978_12
- Patent number
- US04129540
Reaction notes
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