HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → N-[4-(Allylsulfonyl)phenyl]acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 4-(Acetylamino)benzenesulfinic acid | HCID 412150 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-[4-(Allylsulfonyl)phenyl]acetamide | HCID 20375362 | — |
Reaction Steps
50 Parts of p-acetylaminophenylsulfinic acid and 25 parts of sodium hydrogen carbonate are suspended in 300 parts of water. While stirring intensely 36 parts of allyl bromide is dripped in within 3 hours at 50° to 60° C. Stirring is continued for another 4 hours at 60° C. 45 parts of p-allylsulfonylacetanilide is obtained with a melting point of 116° to 118° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04129563 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-b7eadcc681184887b4d6356783e873da |
| Source note | uspto-grants-1978_12 |