HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylamine → 1-Cyclohexyl-3-methylurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-Cyclohexyl-3-methylurea | HCID 308344 | 67.3% |
Reaction Steps
In 500 ml of ethyl ether is dissolved 57 g of methyl isocyanate and, then, 99 g of cyclohexylamine is added dropwise, whereupon crystals separate. The crystals are washed with ether. By the above procedure is obtained 105 g of N-methyl-N'-cyclohexylurea. melting point: 160°-161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04129654 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-764e2897aceb41659d0eff4f06787120 |
| Source note | uspto-grants-1978_12 |