1-Hexanethiol → HCID 178445563, compound

HRID 660175

Reaction equation

HRID 660175 reaction equation
[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:18][CH2:19][N:14]([CH2:15][CH2:16]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH3:5].[CH2:20](S)CCCCC>>[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:18][CH2:19][N:14]([CH2:15][CH2:16]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:20]

Participants

3

Reactant 2

HCID 81061-HexanethiolHCID 178447695HCID 178447695, compound

Product 1

HCID 178445563HCID 178445563, compoundYield 25%

Procedure

Compound 49F was prepared following the procedure as described for the synthesis of compound 49B (see Scheme 10) using hexane-1-thiol as reagent. Subsequent purification by flash chromatography (EtOH) afforded compound 49F.

Workup

  1. customSubsequent purification by flash chromatography (EtOH)

Sources & evidence

ORD record
ord-2240c05a951b4a0c9685379128347196
Source dataset
uspto-grants-2011_12
Patent number
US08084473B2

Linked notes

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