Ammonia → N-methyldihydrophenethylamine

HRID 66397

Reaction equation

HRID 66397 reaction equation
[CH3:1][NH:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.[Li].N>C(O)C>[CH3:1][NH:2][CH2:3][CH2:4][CH:5]1[CH:6]=[CH:7][CH:8]=[CH:9][CH2:10]1

Participants

5

Reactant 3

HCID 222AmmoniaHCID 11503N-MethylbenzeneethanamineHCID 3028194Lithium

Product 1

HCID 21325368N-methyldihydrophenethylamine

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

46 g. (0.34 moles) of N-methylphenethylamine are reduced by treatment with 16 g. of lithium (2.3 g. atom) in 1.5 1. of ammonia and 250 ml. ethanol according to the procedure of Example 1(a) to yield crude N-methyldihydrophenethylamine.

Sources & evidence

ORD record
ord-853d697325634bb4aa8492033409c708
Source dataset
uspto-grants-1978_12
Patent number
US04131744

Linked notes

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