2,6-Dibromonaphthalene → 2-(6-Bromonaphthalene-2-yl)phenanthrene

HRID 68508Notes

Reaction equation

HRID 68508 reaction equation
BrC1C=CC([C:8]2[CH:21]=[CH:20][C:19]3[C:18]4[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=4)[CH:12]=[CH:11][C:10]=3[CH:9]=2)=CC=1.Br[C:23]1[CH:32]=[CH:31][C:30]2[C:25](=[CH:26][CH:27]=[C:28]([Br:33])[CH:29]=2)[CH:24]=1>>[Br:33][C:28]1[CH:29]=[C:30]2[C:25](=[CH:26][CH:27]=1)[CH:24]=[C:23]([C:8]1[CH:21]=[CH:20][C:19]3[C:18]4[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=4)[CH:12]=[CH:11][C:10]=3[CH:9]=1)[CH:32]=[CH:31]2

Participants

3

Reactant 2

HCID 6405912,6-DibromonaphthaleneHCID 581942352-(4-Bromophenyl)phenanthrene

Product 1

HCID 581943962-(6-Bromonaphthalene-2-yl)phenanthrene

Procedure

Synthesis was performed in the same manner as in the synthesis of 2-(4-bromophenyl)phenanthrene except that 2,6-dibromo naphthalene was used instead of 4-bromoiodobenzene.

Workup

  1. customSynthesis

Sources & evidence

ORD record
ord-78ddd11d966f405fb9c0562aea2111f9
Source dataset
uspto-grants-2014_09
Patent number
US08822041B2

Reaction notes

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