HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride, 3,4-dichloro- → 3,4-dichloro-N-[5-chloro-2-(methylthio)phenyl]benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride, 3,4-dichloro- | HCID 7383 | — |
| Reactant | 5-Chloro-2-(methylsulfinyl)aniline | HCID 67972850 | — |
| Product | 3,4-dichloro-N-[5-chloro-2-(methylthio)phenyl]benzenesulfonamide | HCID 67972217 | 21.4% |
Reaction Steps
Following General Procedure B, the title compound (52 mg, 21%) was prepared from 5-chloro-2-(methylsulfinyl)aniline (Intermediate 2) (120 mg, 0.635 mmol) and 3,4-dichlorobenzene-1-sulfonyl chloride (156 mg, 0.635 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822530B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-a6728c0286504da2934217103634da1f |
| Source note | uspto-grants-2014_09 |