HCID 19373362, compound → 2-i-Butyl-2-hydroxymethylpropan-1,3-dithiol

Reaction equation

C([O:8][CH2:9][C:10]([CH2:24][S:25]CC1C=CC=CC=1)([CH2:15][S:16]CC1C=CC=CC=1)[CH2:11][CH:12]([CH3:14])[CH3:13])C1C=CC=CC=1.OCC(CO)(C(C)(C)C)CS>>[CH2:11]([C:10]([CH2:9][OH:8])([CH2:24][SH:25])[CH2:15][SH:16])[CH:12]([CH3:14])[CH3:13]

Participants

Reactant 2

HCID 19373362HCID 19373362, compound

HCID 20075575HCID 20075575, compound

Product 1

HCID 231725902-i-Butyl-2-hydroxymethylpropan-1,3-dithiol

Procedure

2-i-Butyl-2-hydroxymethyl-propan-1,3-dithiol was prepared from 1-benzyloxy-2,2-di-benzylthiomethyl-4-methyl-pentane in a manner analogous to that described for the sysnthesis of 2,2-di-hydroxymethyl-3,3-dimethyl-butan-1-thiol.

Sources & evidence

ORD record: ord-86750268992e4778af76ae1728be1c2d
Source dataset: uspto-grants-1991_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04985582

Reaction notes

Loading…