HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 712927Generated: October 27, 2026
Triphenylphosphine → (9-Carboxynonyl)(triphenyl)phosphanium bromide
https://huagongshe.com/reaction/712927
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 10-Bromodecanoic Acid | HCID 142712 | — |
| Product | (9-Carboxynonyl)(triphenyl)phosphanium bromide | HCID 18795071 | 100% |
Reaction Steps
10-Bromodecanoic acid (19.65 g, 78.24 mmol) and triphenylphosphine (21.45 g, 81.78 mmol) were mixed and stirred at 150° C. for 24 h. Wittig reagent B2 as light yellow syrup was obtained in 100% yield and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09181292B2 |
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| Source dataset | uspto-grants-2015_11 |
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| ORD ID | ord-5b62cc87cd204da78be882dda48f884b |
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| Source note | uspto-grants-2015_11 |
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