HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzyloxyaniline → N-(2-(benzyloxy)phenyl)-3-fluoroisonicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzyloxyaniline | HCID 240548 | — |
| Reactant | 3-Fluoropyridine-4-carboxylic acid | HCID 345361 | — |
| Reactant | 2-(2-Methylsulfanylphenoxy)aniline | HCID 59783707 | — |
| Product | N-(2-(benzyloxy)phenyl)-3-fluoroisonicotinamide | HCID 59783597 | — |
Reaction Steps
Using Procedure S-3 (Table 5) with 3-fluoroisonicotinic acid and 2-(benzyloxy)aniline the title compound 96 was obtained (4.01 g, 88%) as a white solid. MS (m/z): 323.2 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193749B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-4d38487218034f579c9316165d2340d3 |
| Source note | uspto-grants-2015_11 |