Diethyl Ether → HCID 22597223, compound

HRID 7193

Reaction equation

HRID 7193 reaction equation
[CH3:1][C:2]1(O)[CH:9]2[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:11][CH:3]1[CH2:4]3)[CH2:8]2.[C:13](Cl)(=[O:16])[CH:14]=[CH2:15].C([O:20]CC)C>>[C:13]([O:16][C:3]12[CH2:11][CH:7]3[CH2:6][CH:5]([CH2:10][CH:9]([CH2:8]3)[CH:2]1[CH3:1])[CH2:4]2)(=[O:20])[CH:14]=[CH2:15]

Participants

4

Reactant 3

HCID 3283Diethyl EtherHCID 13140Acryloyl chlorideHCID 1365452-Methyl-2-adamantanol

Product 1

HCID 22597223HCID 22597223, compoundYield 55%

Procedure

200 mL of diethyl ether was put into a round-neck flask, 41.5 g of 2-methyl-2-adamantanol and 27.6 g of tetraethyl amine were added thereto and then 22.6 g of acryloyl chloride was dropped. The reactant was reacted at room temperature for about 12 hours and then filtered using diethyl ether. Subsequently, the solvent was removed by an evaporator and then the reactant product was obtained using vacuum distillation (yield: 55%).

Workup

  1. customThe reactant was reacted at room temperature for about 12 hours
  2. filtrationfiltered
  3. customSubsequently, the solvent was removed by an evaporator
  4. customthe reactant product was obtained
  5. distillationvacuum distillation (yield: 55%)

Sources & evidence

ORD record
ord-36f2de1457284bf3b0fda06e472eab7b
Source dataset
uspto-grants-2006_08
Patent number
US07084227B2

Linked notes

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