2,1,3-Benzothiadiazol-5-ylmethanol → 2,1,3-Benzothiadiazole-5-carbaldehyde
Reaction equation
[N:1]1[S:5][N:4]=[C:3]2[CH:6]=[C:7]([CH2:10][OH:11])[CH:8]=[CH:9][C:2]=12>ClCCl.[O-2].[O-2].[Mn+4]>[N:1]1[S:5][N:4]=[C:3]2[CH:6]=[C:7]([CH:10]=[O:11])[CH:8]=[CH:9][C:2]=12Participants
4
Reactant 1
Product 1
Reagents, catalysts & solvents 2
Procedure
This was prepared by oxidation of benzo[1,2,5]thiadiazol-5-yl-methanol (2a) with manganese dioxide in dichloromethane by the method of Example (4c).
Sources & evidence
- ORD record
- ord-c24eaf83cafd42cebb258a0d8ec55660
- Source dataset
- uspto-grants-2006_11
- Patent number
- US07141564B2
Reaction notes
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