Cyanogen Bromide → HCID 178419513, compound

HRID 72378

Reaction equation

[NH2:1][CH2:2][C:3]([NH2:6])([CH3:5])[CH3:4].[N:7]#[C:8][Br:9]>>[BrH:9].[CH3:4][C:3]1([CH3:5])[CH2:2][NH:1][C:8](=[NH:7])[NH:6]1

Participants

Reactant 2

HCID 10476Cyanogen Bromide

HCID 131282-Methylpropylenediamine

Product 1

HCID 178419513HCID 178419513, compoundYield 99.5%

Procedure

The process is carried out according to the procedure described in stage f of Example 1, using 21 g of 1,2-diamino-2-methylpropane and 25.3 g of cyanogen bromide. 46 g of 4,4-dimethylimidazolidin-2-ylideneamine hydrobromide are thus obtained, in the form of a white solid, the characteristics of which are the following:

Sources & evidence

ORD record: ord-55a9b3219e7e4845bb7da11ecdf87d3f
Source dataset: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08828997B2

Linked notes

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