2-(4-Bromophenyl)ethanol → 2-{4-[(7-Nitro-2,3-dihydro-1,4-benzodioxin-6-yl)amino]phenyl}ethanol

HRID 724112

Reaction equation

HRID 724112 reaction equation
[N+:1]([C:4]1[C:5]([NH2:14])=[CH:6][C:7]2[O:12][CH2:11][CH2:10][O:9][C:8]=2[CH:13]=1)([O-:3])=[O:2].Br[C:16]1[CH:21]=[CH:20][C:19]([CH2:22][CH2:23][OH:24])=[CH:18][CH:17]=1>>[N+:1]([C:4]1[C:5]([NH:14][C:16]2[CH:21]=[CH:20][C:19]([CH2:22][CH2:23][OH:24])=[CH:18][CH:17]=2)=[CH:6][C:7]2[O:12][CH2:11][CH2:10][O:9][C:8]=2[CH:13]=1)([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 728512-(4-Bromophenyl)ethanolHCID 6072087-Nitro-2,3-dihydro-1,4-benzodioxin-6-amine

Product 1

HCID 218762872-{4-[(7-Nitro-2,3-dihydro-1,4-benzodioxin-6-yl)amino]phenyl}ethanol

Procedure

The title compound was prepared according to the procedure described in step 1 of Example 45 from 7-nitro-2,3-dihydro-1,4-benzodioxin-6-amine (step 1) and 4-bromophenylethyl alcohol.

Sources & evidence

ORD record
ord-b97fa4ae7f5d49e1bf561eca7af7f0ac
Source dataset
uspto-grants-2006_11
Patent number
US07141580B2

Linked notes

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