HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 4-Nitrodiphenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 1-Chloro-4-nitrobenzene | HCID 7474 | — |
| Reactant | Formanilide | HCID 7671 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | 4-Nitrodiphenylamine | HCID 13271 | — |
Reaction Steps
formanilide method, where formic acid and aniline are used as starting materials to prepare formanilide, which in turn reacts with p-nitro-chlorobenzene in the presence of an acid-binding agent such as potassium carbonate, to produce 4-nitrodiphenylamine, and then, 4-nitrodiphenylamine is reduced by sodium sulfide to form 4-aminodiphenylamine;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07084302B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-7a9eeef338d34ed09b7439bf73611b0e |
| Source note | uspto-grants-2006_08 |