HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-aminoethyl)-4-(1H-imidazol-1-yl)benzamide hydrochloride → N-(2-Aminoethyl)-4-(1H-imidazol-1-yl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-aminoethyl)-4-(1H-imidazol-1-yl)benzamide hydrochloride | HCID 45259278 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(2-Aminoethyl)-4-(1H-imidazol-1-yl)benzamide | HCID 14664358 | — |
Reaction Steps
Dissolve N-(2-aminoethyl)-4-(1H-imidazol-1-yl)benzamide hydrochloride in 50mL H2O and pour onto a column of hydroxide anion exchange resin. Flush the column with H2O and collect fractions with pH>8. Combine the basic fractions and remove the solvents in vacuo to obtain the free base.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05051423 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-b5dab3118b764e1c8e15f1d41f6b4f33 |
| Source note | uspto-grants-1991_09 |